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Title page for etd-0802106-182130


URN etd-0802106-182130 Statistics This thesis had been viewed 2816 times. Download 980 times.
Author Tzu-Chun Hu
Author's Email Address No Public.
Department Chemical Engineering
Year 2005 Semester 2
Degree Master Type of Document Master's Thesis
Language English Page Count 125
Title Use of Design of Experiments to Optimize Scale-up Production of Nanosized Silver Particles
Keyword
  • Experiment Design
  • Scale-up Production
  • Data-driven Model
  • Nanosized Silver Particles
  • Nanosized Silver Particles
  • Data-driven Model
  • Scale-up Production
  • Experiment Design
  • Abstract In our previous work (Lee, 2005), optimization on the synthesis of nanosized silver particles by chemical reduction based on the data-driven model was studied. The results of our previous work were carried out based on the laboratory experimental data (loading 100 cc reacting mixtures in a 200 cc beaker and shaking in an isothermal shaker). In this work, the scale-up production (2 liter or more) of nanosized silver particles is desirable. Extension of the identified data-driven model from the laboratory experimental data to find the optimal operating conditions for scale-up production is achieved by the tailored experiment design. A reliable optimum condition for operating a process can be determined on the basis of the sequential constructed data-driven model originated from the identified model of a small-scale system. Only limited experiments are required. A simulated example and the experimental synthesis of nanosized silver particles were adopted as the testing systems. The proposed heuristic optimization algorithm was examined and proven to be applicable.
    Advisor Committee
  • Jyh-Shyong Chang - advisor
  • Cheng-Liang Chen - co-chair
  • Rong-Chi Wang - co-chair
  • Files indicate accessible at a year
    Date of Defense 2006-07-21 Date of Submission 2006-08-07


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